Data File D:\\AGLIENT 1260\\DATA\\20150825\\20150825 2015-08-25 09-11-32\\BIZ2015-825-DJL1.DSample Name: BIZ2015-825-DJL1=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 63Acq. Instrument : HY-LCMS-02 Location : P1-A-05Injection Date : 8/25/2015 2:33:16 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150825\\20150825 2015-08-25 09-11-32\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 8/25/2015 9:11:33 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\5-80A(RP-HPLC).MLast changed : 8/25/2015 3:25:37 PM by Li Shan(LCMS-02) (modified after loading)Method Info : 10-80A,16MIN Catalog No : HY-B1322 Batch#17631 A-RP-134 Additional Info : Peak(s) manually integrated DAD1 B, Sig=214,4 Ref=off (D:\\AGLIENT...60\\DATA\\20150825\\20150825 2015-08-25 09-11-32\\BIZ2015-825-DJL1.D) 1.420mAU700600500400300200 1.908 2.38310000.511.5 2.99722.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.420 MM 0.0629 2856.84741 756.98798 99.4655 2 1.908 MM 0.0954 4.50603 7.87221e-1 0.1569 3 2.383 MM 0.1679 10.14163 1.00682 0.3531 4 2.997 MM 0.0491 7.04438e-1 2.39225e-1 0.0245 Totals : 2872.19951 759.02124 ===================================================================== *** End of Report ***HY-LCMS-02 8/25/2015 3:25:38 PM Li Shan(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20150825\\20150825 2015-08-25 09-11-32\\BIZ2015-825-DJL1.DSample Name: BIZ2015-825-DJL1=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 63Acq. Instrument : HY-LCMS-02 Location : P1-A-05Injection Date : 8/25/2015 2:33:16 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150825\\20150825 2015-08-25 09-11-32\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 8/25/2015 9:11:33 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\5-80A(RP-HPLC).MLast changed : 8/25/2015 3:26:50 PM by Li Shan(LCMS-02) (modified after loading)Method Info : 10-80A,16MIN Catalog No : HY-B1322 Batch#17631 A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150825\\20150825 2015-08-25 09-11-32\\BIZ2015-825-DJL1.D) ES-API, Pos, Sca 1.4221200000100000080000060000040000020000000.511.522.53min HY-LCMS-02 8/25/2015 3:26:54 PM Li Shan(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20150825\\20150825 2015-08-25 09-11-32\\BIZ2015-825-DJL1.DSample Name: BIZ2015-825-DJL1MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.422 7776846 356.10 I 179.40 I 178.60 I*MSD1 SPC, time=1.397:1.470 of D:\\AGLIENT 1260\\DATA\\20150825\\20150825 2015-08-25 09-11-32\\BIZ2015-825-DJL1.D ES-API,100806040200100150200250300350400m/z 179.4 178.6Max: 604147 *** End of Report ***HY-LCMS-02 8/25/2015 3:26:54 PM Li Shan(LCMS-02) 358.1Page 2 of 2
